2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

Base Information

Chemical Name:2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester
CAS No.:207509-01-1
Molecular Formula:C₄₈H₆₁NO₄
Molecular Weight:716.017
Hs Code.:

Synonyms:2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

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Chemical Property of 2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

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Technology Process of 2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

There total 5 articles about 2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 157999-26-3
myristyl triflate

: 207509-00-0
5-benzyloxy-3-oxo-4S-(tritylamino)pentanoic acid allyl ester

: 207509-01-1
2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 6h;
DOI:10.1021/jo980003i

Reference yield:

: 4726-96-9,32520-12-0
O-Benzyl-L-serine

: 207509-01-1
2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) TMSCl, 2.) Et₃N, 3.) MeOH

2: 1.) CDI / 1.) THF, room temperature, 5 h, 2.) -78 deg C, 30 min; room temperature, 60 min

3: NaH, NaI / tetrahydrofuran; hexamethylphosphoric acid triamide / Heating

With methanol; chloro-trimethyl-silane; sodium hydride; triethylamine; 1,1'-carbonyldiimidazole; sodium iodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jo980003i

Reference yield:

: 76-83-5
trityl chloride

: 207509-01-1
2-[(S)-3-Benzyloxy-2-(trityl-amino)-propionyl]-hexadecanoic acid allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) TMSCl, 2.) Et₃N, 3.) MeOH

2: 1.) CDI / 1.) THF, room temperature, 5 h, 2.) -78 deg C, 30 min; room temperature, 60 min

3: NaH, NaI / tetrahydrofuran; hexamethylphosphoric acid triamide / Heating

With methanol; chloro-trimethyl-silane; sodium hydride; triethylamine; 1,1'-carbonyldiimidazole; sodium iodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jo980003i