Gadolinium tris(1,2,3,4-tetramethylcyclopenta-2,4-dien-1-ide)

Base Information

• Chemical Name: Gadolinium tris(1,2,3,4-tetramethylcyclopenta-2,4-dien-1-ide)
• CAS No.: 308847-85-0
• Molecular Formula: C₂₇H₃₉Gd
• Molecular Weight: 520.857
• DSSTox Substance ID: DTXSID60584093
• Mol file: 308847-85-0.mol

Synonyms:Gadolinium tris(1,2,3,4-tetramethylcyclopenta-2,4-dien-1-ide);gadolinium(3+);1,2,3,5-tetramethylcyclopenta-1,3-diene;DTXSID60584093

Chemical Property of Gadolinium tris(1,2,3,4-tetramethylcyclopenta-2,4-dien-1-ide)

Chemical Property:

• Flash Point: 140 °F
• PSA: 0.00000
• LogP: 7.74570
• Sensitive.: air sensitive, moisture sensitiv
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 521.22929
• Heavy Atom Count: 28
• Complexity: 84.2

Purity/Quality:

99%, ^*data from raw suppliers

Tris(tetramethylcyclopentadienyl)gadolinium(III), min. 98% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F
• Statements: 11-14
• Safety Statements: 7-43

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[C-]1C=C(C(=C1C)C)C.C[C-]1C=C(C(=C1C)C)C.C[C-]1C=C(C(=C1C)C)C.[Gd+3]

Technology Process of Gadolinium tris(1,2,3,4-tetramethylcyclopenta-2,4-dien-1-ide)

There total 1 articles about Gadolinium tris(1,2,3,4-tetramethylcyclopenta-2,4-dien-1-ide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

gadolinium(III) chloride + potassium 2,3,4,5-tetramethyl cyclopentadienyl → Gd(TMCp)3 (308847-85-0)

Guidance literature:

In tetrahydrofuran; at 85 ℃; for 12h; Schlenk technique; Glovebox; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.organomet.8b00557

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