pent-3-yn-1-yl 3-nitrobenzenesulfonate

Base Information

• Chemical Name: pent-3-yn-1-yl 3-nitrobenzenesulfonate
• CAS No.: 17714-50-0
• Molecular Formula: C₁₁H₁₁NO₅S
• Molecular Weight: 269.278
• Mol file: 17714-50-0.mol

Synonyms:pent-3-yn-1-yl 3-nitrobenzenesulfonate

Chemical Property of pent-3-yn-1-yl 3-nitrobenzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of pent-3-yn-1-yl 3-nitrobenzenesulfonate

There total 1 articles about pent-3-yn-1-yl 3-nitrobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

pent-3-yn-1-ol (10229-10-4) + 3-nitrobenzenesulphonyl chloride (121-51-7) → pent-3-yn-1-yl 3-nitrobenzenesulfonate (17714-50-0)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1002/anie.201208197

Reference yield: 50.0%

pent-3-yn-1-yl 3-nitrobenzenesulfonate (17714-50-0) → 2-methylcyclobutanone (1517-15-3)

Guidance literature:

With sodium 2,2,2-trifluoroacetate; trifluoroacetic acid; at 55 ℃; for 120h;

DOI:10.1002/anie.201208197

upstream raw materials:

pent-3-yn-1-ol

3-nitrobenzenesulphonyl chloride

Downstream raw materials:

2-methylcyclobutanone

Refernces