C₁₃H₁₆⁽²⁾H₂N₂

Base Information

Chemical Name:C₁₃H₁₆⁽²⁾H₂N₂
CAS No.:1361111-16-1
Molecular Formula:C₁₃H₁₈N₂
Molecular Weight:204.283
Hs Code.:

C<sub>13</sub>H<sub>16</sub><sup>(2)</sup>H<sub>2</sub>N<sub>2</sub>

Synonyms:C₁₃H₁₆⁽²⁾H₂N₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₆⁽²⁾H₂N₂

Chemical Property:

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Technology Process of C₁₃H₁₆⁽²⁾H₂N₂

There total 4 articles about C₁₃H₁₆⁽²⁾H₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22483-21-2
isobutylidenebenzylamine

: 2206-26-0
[D₃]acetonitrile

: 1361111-16-1
C₁₃H₁₆⁽²⁾H₂N₂

Guidance literature:: [D₃]acetonitrile; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

isobutylidenebenzylamine; In tetrahydrofuran; at -78 ℃; for 4h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; Saturated solution;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 1361111-11-6
C₁₆H₁₃⁽²⁾H₂BrN₂

: 1361111-16-1
C₁₃H₁₆⁽²⁾H₂N₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 0 °C / Reflux

2.1: palladium on activated charcoal; ammonium formate

3.1: potassium carbonate / methanol / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 °C / Inert atmosphere

4.3: Saturated solution

With sulfuric acid; palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 1361110-35-1
methyl 3-(benzylamino)-2,2-dideutero-3-(4-bromophenyl)propanoate

: 1361111-16-1
C₁₃H₁₆⁽²⁾H₂N₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium on activated charcoal; ammonium formate

2.1: potassium carbonate / methanol / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 4 h / -78 °C / Inert atmosphere

3.3: Saturated solution

With palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004