benzyl sinefungin

Base Information

Chemical Name:benzyl sinefungin
CAS No.:1403482-37-0
Molecular Formula:C₂₂H₂₉N₇O₅
Molecular Weight:471.516
Hs Code.:

Synonyms:benzyl sinefungin

Suppliers and Price of benzyl sinefungin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl sinefungin

Chemical Property:

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Technology Process of benzyl sinefungin

There total 7 articles about benzyl sinefungin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: C₃₈H₄₁N₇O₉

: 1403482-37-0
benzyl sinefungin

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic acid; In ethanol; water; for 12h;

Reference yield:

: 1403482-60-9
C₅₀H₅₁N₇O₁₂

: 1403482-37-0
benzyl sinefungin

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 8 h / 22 °C / Inert atmosphere

2: hydrazine hydrate / 8 h / 22 °C / Inert atmosphere

3: palladium on activated carbon; hydrogen / acetic acid / 12 h / Inert atmosphere

With palladium on activated carbon; hydrogen; potassium carbonate; hydrazine hydrate; In methanol; acetic acid;
DOI:10.1021/ja307060p

Reference yield:

: C₄₀H₄₆N₂O₁₃

: 1403482-37-0
benzyl sinefungin

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; lithium hexamethyldisilazane / 3 h / 115 °C / Inert atmosphere

1.2: 2 h / 50 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 8 h / 22 °C / Inert atmosphere

3.1: hydrazine hydrate / 8 h / 22 °C / Inert atmosphere

4.1: palladium on activated carbon; hydrogen / acetic acid / 12 h / Inert atmosphere

With pyridine; palladium on activated carbon; hydrogen; potassium carbonate; hydrazine hydrate; lithium hexamethyldisilazane; In methanol; acetic acid;
DOI:10.1021/ja307060p