diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

Base Information

Chemical Name:diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate
CAS No.:1386395-48-7
Molecular Formula:C₁₄H₂₀Cl₂NO₆P
Molecular Weight:400.196
Hs Code.:

Synonyms:diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

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Chemical Property of diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

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Technology Process of diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

There total 4 articles about diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1386395-40-9
diethyl ((2-((benzyloxy)(methyl)amino)-2-oxoethoxy)(3,4-dichlorophenyl)methyl)phosphonate

: 1386395-48-7
diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 2h; under 760.051 Torr;
DOI:10.1021/jm300652f

Reference yield:

: 1386395-32-9
2-[(3,4-dichlorophenyl)(diethoxyphosphoryl)methoxy]acetic acid

: 1386395-48-7
diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1'-carbonyldiimidazole / dichloromethane / 12 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; 1,1'-carbonyldiimidazole; In dichloromethane; ethyl acetate;
DOI:10.1021/jm300652f

Reference yield:

: 1386395-25-0
benzyl 2-[(3,4-dichlorophenyl)(diethoxyphosphoryl)methoxy]acetate

: 1386395-48-7
diethyl ((3,4-dichlorophenyl)(2-(hydroxy(methyl)amino)-2-oxoethoxy)methyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

2: 1,1'-carbonyldiimidazole / dichloromethane / 12 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With palladium 10% on activated carbon; hydrogen; 1,1'-carbonyldiimidazole; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm300652f