(S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

Base Information

Chemical Name:(S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester
CAS No.:1430195-16-6
Molecular Formula:C₃₆H₃₄O₆
Molecular Weight:562.662
Hs Code.:

Synonyms:(S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

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Technology Process of (S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

There total 3 articles about (S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 19810-31-2
Benzyloxyacetyl chloride

: 1430195-15-5
(S,S)-1,6-diphenyl-hexa-2,4(E,E)-diene-1,6-diol

: 1430195-16-6
(S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo4005074

Reference yield:

: 4187-87-5,61317-73-5,64937-86-6,64599-56-0
1-phenylprop-2-yn-1-ol

: 1430195-16-6
(S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) chloride; N,N,N,N,-tetramethylethylenediamine; oxygen / acetone / 14 h / 40 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3: pyridine / dichloromethane / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; N,N,N,N,-tetramethylethylenediamine; oxygen; copper(l) chloride; In tetrahydrofuran; dichloromethane; acetone; 1: |Glaser Coupling;
DOI:10.1021/jo4005074

Reference yield:

: 197781-95-6
(R,R)-1,6-diphenyl-hexa-2,4-diyne-1,6-diol

: 1430195-16-6
(S,S)-benzyloxyacetic acid 6-(2-benzyloxyacetoxy)-1,6-diphenylhexa-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: pyridine / dichloromethane / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo4005074