diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

Base Information

Chemical Name:diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate
CAS No.:441784-98-1
Molecular Formula:C₂₈H₄₄NO₄PSi
Molecular Weight:517.721
Hs Code.:

Synonyms:diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

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Chemical Property of diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

Chemical Property:

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Technology Process of diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

There total 3 articles about diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134963-85-2
(diisopropoxyphosphoryl)methyl trifluoromethanesulfonate

: 441784-99-2
1-({[t-butyl(diphenyl)silyl]oxy}methyl)-N-methylcyclopropaneamine

: 441784-98-1
diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 441784-97-0
benzyl 1-{[t-butyl(diphenylsilyl)oxy]methylcyclopropyl}(methyl)carbamate

: 441784-98-1
diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 20 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In ethanol; dichloromethane;

Reference yield:

: 441786-55-6
benzyl 1-({[t-butyl(diphenyl)silyl]oxy}methyl)cyclopropylcarbamate

: 441784-98-1
diisopropyl [1-(({[t-butyl(diphenyl)silyl]oxy}(methyl)cyclopropyl)methyl)amino]methylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 4 h / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 20 °C

With hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;