7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

Base Information

Chemical Name:7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene
CAS No.:128957-90-4
Molecular Formula:C₂₀H₂₀BrNO₄
Molecular Weight:418.287
Hs Code.:

Synonyms:7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

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Chemical Property of 7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

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Technology Process of 7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

There total 6 articles about 7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 128957-89-1
7-(6-Bromo-2,3-dimethoxy-benzyl)-5,7,8,9-tetrahydro-1,3-dioxa-7-aza-cyclohepta[f]inden-6-one

: 128957-90-4
7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at -78 ℃;

Reference yield:

: 53811-50-0
6-bromo-2,3-dimethoxybenzaldehyde

: 128957-90-4
7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

Guidance literature:: Multi-step reaction with 5 steps

1: molecular sieves / CH₂Cl₂

2: NaBH₄ / methanol

3: 49 percent / stannic chloride / CH₂Cl₂

4: 98 percent / Zn, acetic acid / Heating

5: 80 percent / diisobutylaluminum hydride / tetrahydrofuran / -78 °C

With sodium tetrahydroborate; molecular sieve; tin(IV) chloride; diisobutylaluminium hydride; acetic acid; zinc; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 128957-87-9
(2-Benzo[1,3]dioxol-5-yl-ethyl)-(6-bromo-2,3-dimethoxy-benzyl)-amine

: 128957-90-4
7-(6-Bromo-2,3-dimethoxy-benzyl)-6,7-dihydro-5H-1,3-dioxa-7-aza-cyclohepta[f]indene

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / stannic chloride / CH₂Cl₂

2: 98 percent / Zn, acetic acid / Heating

3: 80 percent / diisobutylaluminum hydride / tetrahydrofuran / -78 °C

With tin(IV) chloride; diisobutylaluminium hydride; acetic acid; zinc; In tetrahydrofuran; dichloromethane;