Technology Process of C41H59NO5S
There total 17 articles about C41H59NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(1R,2S)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate;
With
triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane;
In
hexane; dichloromethane;
at -78 ℃;
for 2.58333h;
Inert atmosphere;
(2S,4S,6S)-2,4,6,8-tetramethylnonanal;
In
hexane; dichloromethane;
at -78 - 20 ℃;
Inert atmosphere;
DOI:10.1039/c0cc05215a
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: toluene / 4.08 h / 180 °C / Inert atmosphere
2.1: C32H12BF24(1-)*C39H50IrNOP(1+); hydrogen / dichloromethane / 18 h / 20 °C / Autoclave
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere
3.2: Inert atmosphere
4.1: methanol / dichloromethane / 24 h / 20 °C / Inert atmosphere
5.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; acetonitrile / 2 h / 20 °C / Inert atmosphere
6.1: dilithium tetrachlorocuprate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C / Inert atmosphere
6.2: 0.5 h / Inert atmosphere
7.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.17 h / -90 - -78 °C
8.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / hexane; dichloromethane / 2.58 h / -78 °C / Inert atmosphere
8.2: -78 - 20 °C / Inert atmosphere
With
1H-imidazole; methanol; dilithium tetrachlorocuprate; C32H12BF24(1-)*C39H50IrNOP(1+); hydrogen; iodine; sodium hexamethyldisilazane; diisobutylaluminium hydride; triethylamine; triphenylphosphine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; hexane; dichloromethane; toluene; acetonitrile;
1.1: oxy-Cope rearrangement / 8.1: Aldol reaction / 8.2: Aldol reaction;
DOI:10.1039/c0cc05215a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: methanol / dichloromethane / 24 h / 20 °C / Inert atmosphere
3.1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; acetonitrile / 2 h / 20 °C / Inert atmosphere
4.1: dilithium tetrachlorocuprate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C / Inert atmosphere
4.2: 0.5 h / Inert atmosphere
5.1: diisobutylaluminium hydride / hexane; dichloromethane / 2.17 h / -90 - -78 °C
6.1: triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane / hexane; dichloromethane / 2.58 h / -78 °C / Inert atmosphere
6.2: -78 - 20 °C / Inert atmosphere
With
1H-imidazole; methanol; dilithium tetrachlorocuprate; iodine; sodium hexamethyldisilazane; diisobutylaluminium hydride; triethylamine; triphenylphosphine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; diethyl ether; hexane; dichloromethane; acetonitrile;
6.1: Aldol reaction / 6.2: Aldol reaction;
DOI:10.1039/c0cc05215a
