C₆₆H₁₀₆N₆O₂₁

Base Information

Chemical Name:C₆₆H₁₀₆N₆O₂₁
CAS No.:32719-59-8
Molecular Formula:C₆₆H₁₀₆N₆O₂₁
Molecular Weight:1319.6
Hs Code.:

C<sub>66</sub>H<sub>106</sub>N<sub>6</sub>O<sub>21</sub>

Synonyms:C₆₆H₁₀₆N₆O₂₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₆H₁₀₆N₆O₂₁

Chemical Property:

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Technology Process of C₆₆H₁₀₆N₆O₂₁

There total 11 articles about C₆₆H₁₀₆N₆O₂₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.7%

: 5891-45-2
(S)-2-(benzyloxycarbonylamino)pentanedioic acid tert-butyl ester

: 73167-56-3
L-γ-glutamyl-L-γ-glutamyl-L-γ-glutamyl-L-glutamyl-L-glutamic acid hexakis-t-butyl ester

: 32719-59-8
C₆₆H₁₀₆N₆O₂₁

Guidance literature:: (S)-2-(benzyloxycarbonylamino)pentanedioic acid tert-butyl ester; With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 10 - 20 ℃; for 0.5h; Large scale;

L-γ-glutamyl-L-γ-glutamyl-L-γ-glutamyl-L-glutamyl-L-glutamic acid hexakis-t-butyl ester; In dichloromethane; at 20 ℃; for 20h; Large scale;

Reference yield:

: 32719-57-6
tetra-tert-butyl N--L-γ-glutamyl>-L-glutamate

: 32719-59-8
C₆₆H₁₀₆N₆O₂₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / 20 h / 45 °C / Large scale

2.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 10 - 20 °C

2.2: 20 h / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / methanol / 20 h / 45 °C / Large scale

4.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 10 - 20 °C / Large scale

4.2: 20 h / 20 °C / Large scale

5.1: palladium 10% on activated carbon; hydrogen / methanol / 45 °C / Large scale

6.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 10 - 20 °C / Large scale

6.2: 20 h / 20 °C / Large scale

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; HATU; In methanol; dichloromethane;

Reference yield:

: 73167-55-2
L-γ-glutamyl-L-γ-glutamyl-L-γ-glutamic acid tetrakis-t-butyl ester

: 32719-59-8
C₆₆H₁₀₆N₆O₂₁

Guidance literature:: Multi-step reaction with 5 steps

1.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 10 - 20 °C

1.2: 20 h / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 20 h / 45 °C / Large scale

3.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 10 - 20 °C / Large scale

3.2: 20 h / 20 °C / Large scale

4.1: palladium 10% on activated carbon; hydrogen / methanol / 45 °C / Large scale

5.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 10 - 20 °C / Large scale

5.2: 20 h / 20 °C / Large scale

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; HATU; In methanol; dichloromethane;