ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

Base Information

Chemical Name:ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate
CAS No.:125402-10-0
Molecular Formula:C₂₁H₃₀NO₄P
Molecular Weight:391.447
Hs Code.:

Synonyms:ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

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Chemical Property of ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

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Technology Process of ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

There total 1 articles about ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 65600-74-0
ethyl diethoxymethylphosphinate

: 91290-81-2
1,3,5-tris(diphenylmethyl)-hexahydro-1,3,5-triazine

: 125402-10-0
ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1016/S0040-4020(01)89240-1

Reference yield:

: 125402-10-0
ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

: 125402-12-2
ethyl benzhydrylideneaminomethyl(diethoxymethyl)phosphinate

Guidance literature:: With 4 A molecular sieve; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; at 60 ℃; for 1h;
DOI:10.1021/ol990956i

Reference yield:

: 125402-10-0
ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

: 125402-13-3
[1-(Benzhydrylidene-amino)-ethyl]-diethoxymethyl-phosphinic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / H₂ / 5percent Pd/C / ethanol / 20 h / 50 - 60 °C / 38000 - 45600 Torr

2: 82 percent / toluene / 4 h / Heating

3: 1.) BuLi, NH(iPr)2 / 1.) THF, hexane, -78 deg C, 10 min, 2.) THF, hexane, 10 min

4: tetrahydrofuran / 1.) -78 deg C, 2.) 18-24 deg C

With n-butyllithium; hydrogen; diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; toluene;