α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide

Base Information

• Chemical Name: α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide
• CAS No.: 108744-23-6
• Molecular Formula: C₆₁H₈₃N₁₃O₁₃S
• Molecular Weight: 1238.48

Synonyms:α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide

Chemical Property of α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide

Chemical Property:

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Technology Process of α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide

There total 4 articles about α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nα-t-butoxycarbonylaspartic acid α-N-hydroxysuccinimide ester β-benzyl ester (13798-75-9) → α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide (108744-23-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / dimethylformamide

2: H₂ / 10percent Pd/C / dimethylformamide

3: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDAC), 1-hydroxybenzotriazole (HOBt) / dimethylformamide / 0.25 h

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.1021/jm00391a046

Reference yield:

xanthine amine congener (96865-92-8) → α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide (108744-23-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / dimethylformamide

2: H₂ / 10percent Pd/C / dimethylformamide

3: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDAC), 1-hydroxybenzotriazole (HOBt) / dimethylformamide / 0.25 h

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.1021/jm00391a046

Reference yield:

Nα-(tert-butyloxycarbonyl)-α-L-aspartyl-8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine β-benzyl ester (108744-21-4) → α-(tert-butyloxycarbonyl)-α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide (108744-23-6)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / dimethylformamide

2: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDAC), 1-hydroxybenzotriazole (HOBt) / dimethylformamide / 0.25 h

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In N,N-dimethyl-formamide;

DOI:10.1021/jm00391a046

upstream raw materials:

L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine carboxamide hydrochloride

(S)-3-tert-Butoxycarbonylamino-N-(2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-succinamic acid

N^α-t-butoxycarbonylaspartic acid α-N-hydroxysuccinimide ester β-benzyl ester

xanthine amine congener

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