Technology Process of (4S)-4-t-Butyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, Min. 97%
There total 5 articles about (4S)-4-t-Butyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, Min. 97% which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuryl dichloride; N-ethyl-N,N-diisopropylamine;
In
1,2-dichloro-ethane;
at -10 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
With
sodium periodate; ruthenium(III) chloride trihydrate;
In
water; acetonitrile;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/jo902302c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / tetrahydrofuran; water / Cooling with ice
2: thionyl chloride; pyridine / acetonitrile / 3 h / -40 - 20 °C / Inert atmosphere
3: rhodium(III) chloride hydrate; sodium periodate / water; acetonitrile / 1 h / 0 - 20 °C
With
pyridine; sodium periodate; thionyl chloride; rhodium(III) chloride hydrate; sodium carbonate;
In
tetrahydrofuran; water; acetonitrile;
DOI:10.1002/adsc.201500110