N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide

Base Information

Chemical Name:N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide
CAS No.:134168-99-3
Molecular Formula:C₁₁H₁₂Cl₂N₂
Molecular Weight:243.136
Hs Code.:
DSSTox Substance ID:DTXSID201186158
Nikkaji Number:J554.388F

Synonyms:134168-99-3;SCHEMBL9351637;URWSJNMOIUNSQY-UHFFFAOYSA-N;DTXSID201186158;N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide;N-(3,5-Dichlorophenyl)-N'-(tert-butyl)carbodiimide;3,5-Dichloro-N-[(1,1-dimethylethyl)carbonimidoyl]benzenamine

Suppliers and Price of N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide

Chemical Property:

XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:242.0377538
Heavy Atom Count:15
Complexity:254

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)N=C=NC1=CC(=CC(=C1)Cl)Cl

Technology Process of N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide

There total 5 articles about N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 626-43-7
3,5-Dichloroaniline

: 134168-99-3
N-tert-Butyl-N'-(3,5-dichlorophenyl)carbodiimide

Guidance literature:: With 4 A molecular sieve; oxygen; nickel dichloride; In benzene; Heating;
DOI:10.1021/jo00071a021

Reference yield:

: 134168-84-6
N-t-butyl-N'-(3,5-dichlorophenyl)thiourea

: 134168-99-3
N-tert-Butyl-N'-(3,5-dichlorophenyl)carbodiimide

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 50 - 60 ℃;

Reference yield:

: 626-43-7
3,5-Dichloroaniline

: 134168-99-3
N-tert-Butyl-N'-(3,5-dichlorophenyl)carbodiimide

Guidance literature:: Multi-step reaction with 3 steps

1: ethyl acetate / 1.5 h / 75 °C

2: ethyl acetate / 1 h / Ambient temperature

3: dicyclohexylcarbodiimide, Et₃N / tetrahydrofuran / 50 - 60 °C

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;