(Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

Base Information

Chemical Name:(Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester
CAS No.:87227-31-4
Molecular Formula:C₃₅H₄₅O₄P
Molecular Weight:560.714
Hs Code.:

(Triphenyl-λ<sup>5</sup>-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

Synonyms:(Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

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Chemical Property of (Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

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Technology Process of (Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

There total 1 articles about (Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 73818-55-0,15596-07-3
Bestmann ylide

: 87227-18-7
12-[1,3]Dioxolan-2-yl-dodecan-1-ol

: 87227-31-4
(Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

Guidance literature:: In toluene; for 48h; Heating;

Reference yield:

: 87227-31-4
(Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

: 106-02-5,81031-90-5
pentadecanolide

Guidance literature:: Multi-step reaction with 3 steps

1: 0.1 N HCl / Ambient temperature

2: toluene / pH = 8.4; buffer: LiOH, 85percent aq. H₃PO₄, CH₃COOH, B(OH)3

3: 98 percent / H₂ / 5percent Pd/C / ethyl acetate / 3 h / 20 °C / 760 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethyl acetate; toluene;
DOI:10.1055/s-1989-27271

Reference yield:

: 87227-31-4
(Triphenyl-λ⁵-phosphanylidene)-acetic acid 12-[1,3]dioxolan-2-yl-dodecyl ester

: (Triphenyl-λ⁵-phosphanylidene)-acetic acid 13-oxo-tridecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.1 N HCl, THF / 1 h / Ambient temperature

2: LiOH, 85 percent H₃PO₄, glacial acetic acid, B(OH)3 / toluene; H₂O

With tetrahydrofuran; hydrogenchloride; lithium hydroxide; phosphoric acid; boric acid; acetic acid; In water; toluene;