N-benzyloxycarbonyl-L-valyl-L-valine methylamide

Base Information

Chemical Name:N-benzyloxycarbonyl-L-valyl-L-valine methylamide
CAS No.:264887-80-1
Molecular Formula:C₁₉H₂₉N₃O₄
Molecular Weight:363.457
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-valyl-L-valine methylamide

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Chemical Property of N-benzyloxycarbonyl-L-valyl-L-valine methylamide

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Technology Process of N-benzyloxycarbonyl-L-valyl-L-valine methylamide

There total 4 articles about N-benzyloxycarbonyl-L-valyl-L-valine methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 3496-11-5
2,5-dioxopyrrolidin-1-yl (2S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanoate

: 87105-26-8
L-valine N-methylamide

: 264887-80-1
N-benzyloxycarbonyl-L-valyl-L-valine methylamide

Guidance literature:: With triethylamine; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1021/jm990226g

Reference yield:

: C₁₈H₂₅NO₅

: 264887-80-1
N-benzyloxycarbonyl-L-valyl-L-valine methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / tetrahydrofuran / 20 °C

2: 98 percent / H₂ / Pd/C / methanol / 3 h / 25 °C / 1551.49 Torr

3: 58 percent / Et₃N / H₂O; tetrahydrofuran / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; water; 1: Condensation / 2: Hydrogenolysis / 3: Condensation;
DOI:10.1021/jm990226g

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 264887-80-1
N-benzyloxycarbonyl-L-valyl-L-valine methylamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-ethylmorpholine / tetrahydrofuran / 0.5 h / -10 °C

2: 68 percent / tetrahydrofuran / 20 °C

3: 98 percent / H₂ / Pd/C / methanol / 3 h / 25 °C / 1551.49 Torr

4: 58 percent / Et₃N / H₂O; tetrahydrofuran / 20 °C

With N-ethylmorpholine;; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; water; 1: Acylation / 2: Condensation / 3: Hydrogenolysis / 4: Condensation;
DOI:10.1021/jm990226g