(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

Base Information

Chemical Name:(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro
CAS No.:160728-72-3
Molecular Formula:C₂₂H₃₃NS₂
Molecular Weight:375.643
Hs Code.:

(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro<decahydroquinoline-6-2'-1',3'-dithiolane>

Synonyms:(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

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Technology Process of (2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

There total 1 articles about (2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 540-63-6
ethane-1,2-dithiol

: (1S,4aS,5RS,8aR)-1-Benzyl-5-methyl-2-propyldecahydroquinolin-6-one

: 160728-72-3
(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

Guidance literature:: With zinc trifluoromethanesulfonate; 1.) CH₂Cl₂, reflux, 4 d; 2.) reflux 4 d;
DOI:10.1016/0040-4039(94)88469-2

Reference yield: 68.0%

: 160728-72-3
(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

: 160798-33-4
(2S,4aS,5R,8aR)-1-Benzyl-5-methyl-2-propyldecahydroquinoline

Guidance literature:: With nickel; In 1,4-dioxane; Heating;
DOI:10.1016/0040-4039(94)88469-2

Reference yield:

: 160728-72-3
(2S,4aS,5S,8aR)-1-Benzyl-5-methyl-2-propylspiro

: 27766-71-8
(-)-pumiliotoxin C

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Raney Ni / dioxane / Heating

2: 92 percent / hydrogen / 10percent Pd/C / methanol

With hydrogen; nickel; palladium on activated charcoal; In 1,4-dioxane; methanol;
DOI:10.1016/0040-4039(94)88469-2