C₉H₇ClF₃N₃*ClH

Base Information

• Chemical Name: C₉H₇ClF₃N₃*ClH
• CAS No.: 1309044-55-0
• Molecular Formula: C₉H₇ClF₃N₃*ClH
• Molecular Weight: 286.084
• Mol file: 1309044-55-0.mol

Synonyms:C₉H₇ClF₃N₃*ClH

Chemical Property of C₉H₇ClF₃N₃*ClH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₇ClF₃N₃*ClH

There total 2 articles about C₉H₇ClF₃N₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C9H7ClF3N3 (1309044-51-6) → C9H7ClF3N3*ClH (1309044-55-0)

Guidance literature:

With hydrogenchloride; In diethyl ether; Inert atmosphere;

DOI:10.1021/ic2003996

Reference yield:

p-chlorobenzamidine (19563-04-3) → C9H7ClF3N3*ClH (1309044-55-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / -196 - 60 °C / Inert atmosphere

2: hydrogenchloride / diethyl ether / Inert atmosphere

With hydrogenchloride; In diethyl ether; acetonitrile;

DOI:10.1021/ic2003996

Reference yield: 99.0%

C9H7ClF3N3*ClH (1309044-55-0) → C9H4Cl2F3N3S (1308251-17-3)

Guidance literature:

With sulfur dichloride; In acetonitrile; Reflux; Inert atmosphere;

DOI:10.1021/ic2003996

upstream raw materials:

C₉H₇ClF₃N₃

p-chlorobenzamidine

Downstream raw materials:

C₉H₄Cl₂F₃N₃S

C₉H₄ClF₃N₃S