Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

Base Information

Chemical Name:Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)
CAS No.:1569084-21-4
Molecular Formula:C₄₇H₃₉CuN₄O₄
Molecular Weight:787.397
Hs Code.:

Synonyms:Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

Suppliers and Price of Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

There total 2 articles about Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.3%

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 144342-50-7
Diethyl 6,6'-dimethyl-2,2'-bipyridine-4,4'-dicarboxylate

: 18120-22-4
1,13-diphenyl-6,8-diisoindolemethene

: 1569084-21-4
Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

Guidance literature:: tetrakis(acetonitrile)copper(I)tetrafluoroborate; 1,13-diphenyl-6,8-diisoindolemethene; With sodium hydroxide; In water; acetone; at 20 ℃; for 0.166667h; Inert atmosphere;

Diethyl 6,6'-dimethyl-2,2'-bipyridine-4,4'-dicarboxylate; In water; acetone; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c3dt53334d

Reference yield:

: 144342-49-4
6,6′-dimethyl-2,2′-bipyridine-4,4′-dicarboxylic acid

: 1569084-21-4
Cu(1,13-diphenyl-6,8-diisoindolemethene-H)(4,4’-(CO2Et)-6,6’-dimethyl-2,2’-bipyridine)

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 72 h / Reflux; Inert atmosphere

2.1: sodium hydroxide / water; acetone / 0.17 h / 20 °C / Inert atmosphere

2.2: 1.5 h / 20 °C / Inert atmosphere

With sulfuric acid; sodium hydroxide; In water; acetone;
DOI:10.1039/c3dt53334d