Technology Process of C57H73N13O11
There total 3 articles about C57H73N13O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-[3-tert-butoxycarbonylamino-5,7-bis-(2-carboxy-ethyl)-adamantan-1-yl]-propionic acid;
With
N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.166667h;
L-azidohomoalanine benzyl ester hydrochloride;
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 72h;
DOI:10.1002/ejoc.201300769
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloromethane / 1.5 h / 20 °C
2.1: hydrogenchloride; water / tetrahydrofuran
3.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h / 0 °C
3.2: 72 h / 0 - 20 °C
With
hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201300769
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride; water / tetrahydrofuran
2.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h / 0 °C
2.2: 72 h / 0 - 20 °C
With
hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201300769
