2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether

Base Information

Chemical Name:2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether
CAS No.:887757-58-6
Molecular Formula:C₁₈H₁₉BrN₂O₂
Molecular Weight:375.265
Hs Code.:

Synonyms:2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether

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Chemical Property of 2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether

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Technology Process of 2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether

There total 2 articles about 2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.7%

: 56256-14-5
4-bromo-3-methoxy-benzoic acid

: 40358-34-7
2-methyl-2,3,4,5-tetrahydro-1H-benzo[b] [1,4] diazepine

: 887757-58-6
2-bromo-5-[(4-methyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)carbonyl]phenyl methyl ether

Guidance literature:: 4-bromo-3-methoxy-benzoic acid; With thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 20 ℃; for 3h;

2-methyl-2,3,4,5-tetrahydro-1H-benzo[b] [1,4] diazepine; With pyridine; In tetrahydrofuran; at 20 ℃; for 2h;