1,6-N-(benzyloxycarbonyl)aza[60]fulleroid

Base Information

• Chemical Name: 1,6-N-(benzyloxycarbonyl)aza[60]fulleroid
• CAS No.: 1117893-99-8
• Molecular Formula: C₆₈H₇NO₂
• Molecular Weight: 869.809

Synonyms:1,6-N-(benzyloxycarbonyl)aza[60]fulleroid

Chemical Property of 1,6-N-(benzyloxycarbonyl)aza[60]fulleroid

Chemical Property:

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Technology Process of 1,6-N-(benzyloxycarbonyl)aza[60]fulleroid

There total 2 articles about 1,6-N-(benzyloxycarbonyl)aza[60]fulleroid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

1,2-N-(benzyloxycarbonyl)aziridino[60]fullerene (1117893-82-9) → 1,6-N-(benzyloxycarbonyl)aza[60]fulleroid (1117893-99-8)

Guidance literature:

With chloramine B; In toluene; for 6h; Inert atmosphere; Reflux;

DOI:10.1021/jo8025737

Reference yield: 29.2%

O-benzyl carbamate (621-84-1) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 1,6-N-(benzyloxycarbonyl)aza[60]fulleroid (1117893-99-8)

Guidance literature:

With N-iodo-succinimide; In 1,2-dichloro-benzene; at 80 ℃; for 6h;

DOI:10.1039/c7ob01347g

Reference yield: 6.8%

1,6-N-(benzyloxycarbonyl)aza[60]fulleroid (1117893-99-8) → C68H7NO4

Guidance literature:

With oxygen; In 1,2-dichloro-benzene; for 30h; Irradiation;

DOI:10.1039/c7ob01347g

upstream raw materials:

1,2-N-(benzyloxycarbonyl)aziridino[60]fullerene

O-benzyl carbamate

fullerene-C₆₀

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