di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium

Base Information

• Chemical Name: di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium
• CAS No.: 1273319-63-3
• Molecular Formula: C₃₆H₆₆Be₂Cl₄P₂
• Molecular Weight: 720.704
• Mol file: 1273319-63-3.mol

Synonyms:di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium

Chemical Property of di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium

Chemical Property:

Purity/Quality:

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Technology Process of di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium

There total 1 articles about di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

beryllium(II) chloride (7787-47-5) + palladium(0)bis(tricyclohexylphosphine) (33309-88-5) → di-μ-chloro-trans-dichlorobis(tricyclohexylphosphine)diberyllium (1273319-63-3) + palladium (7440-05-3)

Guidance literature:

In toluene; (Ar), small excess of BeCl2 added to soln. of Pd complex in toluene, heated at 80°C for 18 h, asecond portion of BeCl2 added, heated at 80°C for 18 h; filtered, layered (hexane), evapd. at room temp., redissolved (C6D6), elem. anal.;

DOI:10.1515/znb-2011-0109

upstream raw materials:

beryllium(II) chloride

palladium⁽⁰⁾bis(tricyclohexylphosphine)