(4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane
CAS No.:1415692-93-1
Molecular Formula:C₂₉H₄₉BO₄Si
Molecular Weight:500.602
Hs Code.:

Synonyms:(4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

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Technology Process of (4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

There total 2 articles about (4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 304915-07-9
[2(1R),4S,5S]-4,5-dicyclohexyl-2-[1-chloro-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-1,3,2-dioxaborolane

: 100-51-6,185532-71-2
benzyl alcohol

: 1415692-93-1
(4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; Reflux;
DOI:10.1039/c2ob26756j

Reference yield:

: 304915-06-8
(4S,5S)-4,5-dicyclohexyl-2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl-1,3,2-dioxaborolane

: 1415692-93-1
(4S,5S)-2-[(1S)-2-[(tert-butyldimethylsilyl)oxy]-1-(benzyloxy)ethyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: zinc(II) chloride; n-butyllithium; dichloromethane / hexane; tetrahydrofuran; diethyl ether / 20 °C

2: sodium hydride / tetrahydrofuran; mineral oil / Reflux

With n-butyllithium; dichloromethane; sodium hydride; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; mineral oil;
DOI:10.1039/c2ob26756j