C₂₃H₂₄N₂O₂S

Base Information

Chemical Name:C₂₃H₂₄N₂O₂S
CAS No.:1451192-94-1
Molecular Formula:C₂₃H₂₄N₂O₂S
Molecular Weight:392.522
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₂₃H₂₄N₂O₂S

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Chemical Property of C₂₃H₂₄N₂O₂S

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Technology Process of C₂₃H₂₄N₂O₂S

There total 8 articles about C₂₃H₂₄N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1451192-89-4
C₂₇H₃₂N₂O₃S₂

: 1451192-94-1
C₂₃H₂₄N₂O₂S

Guidance literature:: With hydrogenchloride; In methanol; water; at 0 ℃; Inert atmosphere;
DOI:10.1021/ja408114u

Reference yield:

: 1451192-91-8
C₂₆H₃₂N₂O₅S₂

: 1451192-94-1
C₂₃H₂₄N₂O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide / 0.67 h / -15 °C / Inert atmosphere

1.2: 2 h / -15 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 - 0 °C / Inert atmosphere

4.2: 2 h / -78 - 20 °C / Inert atmosphere

5.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 48 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride / methanol; water / 0 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja408114u

Reference yield:

: 1451192-86-1
C₂₉H₃₆N₂O₅S₂

: 1451192-94-1
C₂₃H₂₄N₂O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 - 0 °C / Inert atmosphere

3.2: 2 h / -78 - 20 °C / Inert atmosphere

4.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 48 h / 20 °C / Inert atmosphere

5.1: hydrogenchloride / methanol; water / 0 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; Hoveyda-Grubbs catalyst second generation; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/ja408114u