1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

Base Information

Chemical Name:1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone
CAS No.:136616-28-9
Molecular Formula:C₁₅H₁₉ClO₄
Molecular Weight:298.766
Hs Code.:

Synonyms:1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

Suppliers and Price of 1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

Chemical Property:

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Technology Process of 1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

There total 3 articles about 1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 35666-69-4
(2R,3E)-3-penten-2-ol

: 81325-85-1
3'-chloro-2'-hydroxy-4',6'-dimethoxyacetophenone

: 136616-28-9
1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

Guidance literature:: With tributylphosphine; di-isopropyl azodicarboxylate;
DOI:10.1021/ja00022a075

Reference yield:

: 18113-21-8
chloroglucinol dimethyl ether

: 136616-28-9
1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine

2: 94 percent / AlCl₃ / chlorobenzene / 0.5 h / Heating

3: 73 percent / diisopropylazodicarboxylate, tributylphosphine

With pyridine; aluminium trichloride; tributylphosphine; di-isopropyl azodicarboxylate; In chlorobenzene;
DOI:10.1021/ja00022a075

Reference yield:

: 131939-10-1
Acetic acid 2-chloro-3,5-dimethoxy-phenyl ester

: 136616-28-9
1-[3-Chloro-4,6-dimethoxy-2-((E)-(S)-1-methyl-but-2-enyloxy)-phenyl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / AlCl₃ / chlorobenzene / 0.5 h / Heating

2: 73 percent / diisopropylazodicarboxylate, tributylphosphine

With aluminium trichloride; tributylphosphine; di-isopropyl azodicarboxylate; In chlorobenzene;
DOI:10.1021/ja00022a075