2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

Base Information

Chemical Name:2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol
CAS No.:1438868-11-1
Molecular Formula:C₂₁H₂₆O₄S
Molecular Weight:374.501
Hs Code.:

Synonyms:2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

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Chemical Property of 2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

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Technology Process of 2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

There total 9 articles about 2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 1438868-05-3
2-(benzyloxy)-4-(ethylthio)-6-(hydroxymethyl)phenol

: 1438868-11-1
2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

Guidance literature:: 2-(benzyloxy)-4-(ethylthio)-6-(hydroxymethyl)phenol; With toluene-4-sulfonic acid; In dichloromethane; at -10 ℃; for 0.25h; Inert atmosphere;

3,4-dihydro-2H-pyran; In dichloromethane; at 25 ℃; Inert atmosphere;
DOI:10.1002/cjoc.201200977

Reference yield:

: C₁₇H₁₈O₃S

: 1438868-11-1
2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 25 °C / Inert atmosphere

2.1: water; hydrogenchloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

3.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

With hydrogenchloride; water; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.201200977

Reference yield:

: 1438867-92-5
2-(benzyloxy)-6-(hydroxymethyl)-4-iodophenol

: 1438868-11-1
2-(benzyloxy)-4-(ethylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2.1: potassium carbonate; copper(l) iodide; sulfur / N,N-dimethyl-formamide / 10 h / 90 °C / Inert atmosphere

2.2: 40 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide / 25 °C / Inert atmosphere

4.1: water; hydrogenchloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

5.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

5.2: 25 °C / Inert atmosphere

With hydrogenchloride; copper(l) iodide; water; potassium carbonate; toluene-4-sulfonic acid; sulfur; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.201200977