Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

Base Information

Chemical Name:Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;
CAS No.:143023-21-6
Molecular Formula:CH₃O₃S*C₃₀H₂₉N₅O₂P
Molecular Weight:617.665
Hs Code.:

Synonyms:Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

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Chemical Property of Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

Chemical Property:

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Technology Process of Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

There total 3 articles about Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 143023-18-1
Methanesulfonic acid 2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl ester

: 603-35-0
triphenylphosphine

: 143023-21-6
Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

Guidance literature:: In acetonitrile; at 90 ℃;
DOI:10.1016/S0040-4039(00)92091-4

Reference yield:

: 143023-19-2
Potassium; 2-(2,2-dimethyl-propionylamino)-6-hydroxymethyl-pteridin-4-olate

: 143023-21-6
Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N / CH₂Cl₂ / 0 °C

2: 76 percent / acetonitrile / 90 °C

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)92091-4

Reference yield:

: 142645-51-0
6-pivaloyloxymethyl-2-pivaloylaminopteridin-4(3H)-one

: 143023-21-6
Methanesulfonate[2-(2,2-dimethyl-propionylamino)-4-oxo-3,4-dihydro-pteridin-6-ylmethyl]-triphenyl-phosphonium;

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / K₂CO₃ / methanol

2: 72 percent / Et₃N / CH₂Cl₂ / 0 °C

3: 76 percent / acetonitrile / 90 °C

With potassium carbonate; triethylamine; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4039(00)92091-4