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C35H48N8O4

Base Information
  • Chemical Name:C35H48N8O4
  • CAS No.:1346245-79-1
  • Molecular Formula:C35H48N8O4
  • Molecular Weight:644.817
  • Hs Code.:
C<sub>35</sub>H<sub>48</sub>N<sub>8</sub>O<sub>4</sub>

Synonyms:C35H48N8O4

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Chemical Property of C35H48N8O4
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Technology Process of C35H48N8O4

There total 7 articles about C35H48N8O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In acetonitrile; at 100 ℃; for 12h; sealed vessel;
Guidance literature:
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetonitrile / 12 h / 90 °C
2.1: triethylamine / dmap / dichloromethane / 18 h / 5 - 20 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
3.2: Cooling with ice
4.1: triethylamine / dichloromethane / 2 h / 5 - 10 °C / Inert atmosphere
5.1: acetonitrile / 12 h / 100 °C / sealed vessel
With tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; dmap; In tetrahydrofuran; dichloromethane; acetonitrile;
Guidance literature:
Multi-step reaction with 7 steps
1.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium(0); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 1,4-dioxane; water / 15 h / 80 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 10 °C
2.2: 1 h / 20 °C / Inert atmosphere
3.1: potassium carbonate / acetonitrile / 12 h / 90 °C
4.1: triethylamine / dmap / dichloromethane / 18 h / 5 - 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C
5.2: Cooling with ice
6.1: triethylamine / dichloromethane / 2 h / 5 - 10 °C / Inert atmosphere
7.1: acetonitrile / 12 h / 100 °C / sealed vessel
With potassium phosphate; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triethylamine; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dmap; tris-(dibenzylideneacetone)dipalladium(0); In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
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