C₆₄H₇₆O₁₁SSi

Base Information

Chemical Name:C₆₄H₇₆O₁₁SSi
CAS No.:1265446-66-9
Molecular Formula:C₆₄H₇₆O₁₁SSi
Molecular Weight:1081.45
Hs Code.:

C<sub>64</sub>H<sub>76</sub>O<sub>11</sub>SSi

Synonyms:C₆₄H₇₆O₁₁SSi

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Chemical Property of C₆₄H₇₆O₁₁SSi

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Technology Process of C₆₄H₇₆O₁₁SSi

There total 3 articles about C₆₄H₇₆O₁₁SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1265446-63-6
C₇₀H₈₀O₁₁SSeSi

: 1265446-66-9
C₆₄H₇₆O₁₁SSi

: 1265446-69-2
C₆₄H₇₆O₁₁SSi

Guidance literature:: With triethyl borane; tri-n-butyl-tin hydride; In benzene; at 20 ℃; optical yield given as %de; stereoselective reaction; in air;
DOI:10.1021/np100729d

Reference yield:

: 1265446-53-4
C₆₇H₈₆O₁₀SeSi₂

: 1265446-66-9
C₆₄H₇₆O₁₁SSi

: 1265446-69-2
C₆₄H₇₆O₁₁SSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / -30 - 0 °C

2.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C

2.2: Inert atmosphere

3.1: triethyl borane; tri-n-butyl-tin hydride / benzene / 20 °C / in air

With triethyl borane; tetrabutyl ammonium fluoride; methyllithium; tri-n-butyl-tin hydride; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/np100729d

Reference yield:

: 1265446-57-8
C₆₁H₇₂O₁₀SeSi

: 1265446-66-9
C₆₄H₇₆O₁₁SSi

: 1265446-69-2
C₆₄H₇₆O₁₁SSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C

1.2: Inert atmosphere

2.1: triethyl borane; tri-n-butyl-tin hydride / benzene / 20 °C / in air

With triethyl borane; methyllithium; tri-n-butyl-tin hydride; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/np100729d