3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol

Base Information

Chemical Name:3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol
CAS No.:1310059-30-3
Molecular Formula:C₂₁H₂₄O₂
Molecular Weight:308.42
Hs Code.:

Synonyms:3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol

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Technology Process of 3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol

There total 1 articles about 3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1310059-47-2
1-phenethyl-3-phenyl-2-propynyl 2-bromo-2-methylpropanoate

: 1310059-30-3
3,3-dimethyl-5-phenethyl-4-[(E)-1-phenylmethylidene]tetrahydro-2-furanol

Guidance literature:: 1-phenethyl-3-phenyl-2-propynyl 2-bromo-2-methylpropanoate; With diisobutylaluminium hydride; In toluene; at -78 ℃; for 0.25h; Inert atmosphere;

With triethyl borane; tri-n-butyl-tin hydride; In hexane; toluene; at -78 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201100049