3-fluoro-1-phenylenyne

Base Information

Chemical Name:3-fluoro-1-phenylenyne
CAS No.:1432736-74-7
Molecular Formula:C₁₀H₇F
Molecular Weight:146.164
Hs Code.:

Synonyms:3-fluoro-1-phenylenyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-fluoro-1-phenylenyne

Chemical Property:

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Technology Process of 3-fluoro-1-phenylenyne

There total 1 articles about 3-fluoro-1-phenylenyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 420-25-7
1-bromo-1-fluoroethylene

: 536-74-3
phenylacetylene

: 1432736-74-7
3-fluoro-1-phenylenyne

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; Schlenk technique; Inert atmosphere; Cooling with acetone-dry ice;
DOI:10.1021/ol401057z

Reference yield: 85.0%

: 886-66-8
1,4-diphenyl-1,3-butadiyne

: 1432736-74-7
3-fluoro-1-phenylenyne

: 1432736-48-5
C₂₆H₁₇F

Guidance literature:: With allylchloro[1,3-bis(2,6-di-isopropylphenyl)imidazol-2-ylidine]palladium(II); trifuran-2-yl-phosphane; cesium pivalate; In toluene; at 120 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol401057z

Reference yield: 69.0%

: 1432736-74-7
3-fluoro-1-phenylenyne

: dimethyl 4,4′-(buta-1,3-diyne-1,4-diyl)dibenzoate

: 1432736-59-8
C₃₀H₂₁FO₄

Guidance literature:: With allylchloro[1,3-bis(2,6-di-isopropylphenyl)imidazol-2-ylidine]palladium(II); trifuran-2-yl-phosphane; cesium pivalate; In toluene; at 120 ℃; for 16h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol401057z