N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

Base Information

Chemical Name:N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine
CAS No.:1269205-85-7
Molecular Formula:C₂₅H₂₆N₆O
Molecular Weight:426.521
Hs Code.:

Synonyms:N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

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Technology Process of N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

There total 1 articles about N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1204-86-0
4-(4-morpholinyl)benzaldehyde

: 1197040-29-1,931-54-4
phenyl isocyanate

: 100-46-9
benzylamine

: 1269205-85-7
N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

Guidance literature:: With trimethylsilylazide; In methanol; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1055/s-0030-1258273

Reference yield: 92.0%

: 1269205-85-7
N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

: 1269205-92-6
(4-morpholinophenyl)(1-phenyl-1H-tetrazol-5-yl)methanamine

Guidance literature:: With 10% palladium on activated carbon; hydrogen; In methanol; at 60 ℃; for 24h;
DOI:10.1055/s-0030-1258273

Reference yield:

: 1269205-85-7
N-benzyl-1-(4-morpholinophenyl)-1-(1-phenyl-1H-tetrazol-5-yl)methanamine

: C₆H₅O₃S^(1-)*C₂₅H₂₆N₇O⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated carbon; hydrogen / methanol / 24 h / 60 °C

2: dichloromethane; N,N-dimethyl-formamide / 8 h / 20 °C

With 10% palladium on activated carbon; hydrogen; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0030-1258273