Technology Process of N-Methyl-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin
There total 8 articles about N-Methyl-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
under 760 - 3040 Torr;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 88 percent / NH4OAc / 5 h / Heating
2: LiAlH4 / diethyl ether / 48 h / Ambient temperature
3: 87 percent / 1 h / 100 °C
4: 67 percent / 2.) HCl / benzene / 6 h / Heating
5: 89 percent / H2 / 10percent Pd/C / tetrahydrofuran / 760 - 3040 Torr / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; ammonium acetate; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 81 percent / SOCl2 / diethyl ether / 3 h / Heating
2: 65 percent / DMSO / 3 h / 40 °C
3: LiAlH4 / diethyl ether / 48 h / Ambient temperature
4: 87 percent / 1 h / 100 °C
5: 67 percent / 2.) HCl / benzene / 6 h / Heating
6: 89 percent / H2 / 10percent Pd/C / tetrahydrofuran / 760 - 3040 Torr / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; hydrogen; dimethyl sulfoxide;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; benzene;