Technology Process of 2,4-dimethoxy-6-(2'-hydroxy)ethylphenol
There total 5 articles about 2,4-dimethoxy-6-(2'-hydroxy)ethylphenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dichloromethane;
at 0 - 20 ℃;
for 1h;
DOI:10.1021/jo000696e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N,N-diethylaniline / 4 h / Heating
2.1: triethylamine / CH2Cl2 / 0 - 20 °C
3.1: OsO4; NaIO4 / diethyl ether; acetone; H2O / 8 h
3.2: sodium borohydride / methanol / 0.5 h / 0 °C
4.1: tetra-n-butylammonium fluoride / CH2Cl2; tetrahydrofuran / 1 h / 0 - 20 °C
With
sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; triethylamine; N,N-diethylaniline;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; acetone;
2.1: Claisen rearrangement;
DOI:10.1021/jo000696e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / CH2Cl2 / 0 - 20 °C
2.1: OsO4; NaIO4 / diethyl ether; acetone; H2O / 8 h
2.2: sodium borohydride / methanol / 0.5 h / 0 °C
3.1: tetra-n-butylammonium fluoride / CH2Cl2; tetrahydrofuran / 1 h / 0 - 20 °C
With
sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; acetone;
DOI:10.1021/jo000696e
![2-[2-(<i>tert</i>-butyl-dimethyl-silanyloxy)-3,5-dimethoxy-phenyl]-ethanol](/Databaselist/images/loading.webp)
