N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

Base Information

Chemical Name:N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide
CAS No.:73365-46-5
Molecular Formula:C₁₈H₂₄N₂O₃
Molecular Weight:316.4
Hs Code.:

Synonyms:N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

Chemical Property:

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Technology Process of N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

There total 11 articles about N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73331-65-4
N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-N-((R)-1-phenyl-ethyl)-benzamide

: 73365-46-5
N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

Guidance literature:: With formic acid; at 40 - 50 ℃;
DOI:10.1021/ja00522a095

Reference yield:

: 67492-40-4
2,5-Anhydro-4,6-di-Se-phenyl-4,6-diseleno-L-mannose Dimethyl Acetal

: 73365-46-5
N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / W-4 Raney nickel / tetrahydrofuran / 25 °C

2: pyridine / 0 °C

3: sodium methylate / methanol / Heating

4: TsOH / tetrahydrofuran / Heating

5: methanol / 25 °C

6: 95percent formic acid / 40 - 50 °C

With pyridine; formic acid; W-4 Raney nickel; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol;
DOI:10.1021/ja00522a095

Reference yield:

: 39022-34-9
3,6-di-O-p-tolylsulfonyl-2,5-anhydro-L-idofuranose dimethylacetal

: 73365-46-5
N-[(R)-tert-Butylcarbamoyl-((2R,5S)-5-methyl-2,5-dihydro-furan-2-yl)-methyl]-benzamide

Guidance literature:: Multi-step reaction with 8 steps

1: 93 percent / sodium hydride / tetrahydrofuran / 25 °C

2: dimethylformamide / Heating

3: 96 percent / W-4 Raney nickel / tetrahydrofuran / 25 °C

4: pyridine / 0 °C

5: sodium methylate / methanol / Heating

6: TsOH / tetrahydrofuran / Heating

7: methanol / 25 °C

8: 95percent formic acid / 40 - 50 °C

With pyridine; formic acid; W-4 Raney nickel; sodium methylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00522a095