1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

Base Information

Chemical Name:1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine
CAS No.:137248-61-4
Molecular Formula:C₂₃H₂₄FN₂O₆P
Molecular Weight:474.426
Hs Code.:

Synonyms:1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

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Chemical Property of 1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

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Technology Process of 1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

There total 4 articles about 1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 137248-60-3
1-(2',3',5',6'-tetradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hex-5'-enofuranosyl)thymine

: 137248-61-4
1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 6h; under 760 Torr;

Reference yield:

: 22400-41-5
diphenyl [(triphenylphosphoranylidene)methyl]phosphonate

: 137248-61-4
1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfoxide / 24 h / Ambient temperature

2: 90 percent / H₂ / 10percent Pd/C / ethanol / 6 h / 760 Torr

With hydrogen; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;

Reference yield:

: 137248-59-0
(2R,3S,5R)-3-Fluoro-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-carbaldehyde

: 137248-61-4
1-(2',3',5',6'-teradeoxy-3'-fluoro-6'-diphenoxyphosphoryl-β-D-erythro-hexafuranosyl)thymine

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfoxide / 24 h / Ambient temperature

2: 90 percent / H₂ / 10percent Pd/C / ethanol / 6 h / 760 Torr

With hydrogen; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;