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Technology Process of (C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6

(C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6

Base Information
  • Chemical Name:(C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6
  • CAS No.:79919-53-2
  • Molecular Formula:C31H31N2OPRe*F6P
  • Molecular Weight:809.745
  • Hs Code.:
(C<sub>5</sub>H<sub>5</sub>)ReNO{P(C<sub>6</sub>H<sub>5</sub>)3}(CH<sub>2</sub>(CH<sub>3</sub>)2NC<sub>5</sub>H<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>)ReNOP(C<sub>6</sub>H<sub>5</sub>)3CH<sub>2</sub>(CH<sub>3</sub>)2NC<sub>5</sub>H<sub>3</sub>PF<sub>6</sub>

Synonyms:(C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6

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Chemical Property of (C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6
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Technology Process of (C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6

There total 1 articles about (C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,6-dimethylpyridine
108-48-5

2,6-dimethylpyridine

(η5-C5H5)(Me)(NO)(PPh3)rhenium(II)

(η5-C5H5)(Me)(NO)(PPh3)rhenium(II)

tritylium hexafluorophosphate
437-17-2

tritylium hexafluorophosphate

(C<sub>5</sub>H<sub>5</sub>)ReNO{P(C<sub>6</sub>H<sub>5</sub>)3}(CH<sub>2</sub>(CH<sub>3</sub>)2NC<sub>5</sub>H<sub>3</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>)ReNOP(C<sub>6</sub>H<sub>5</sub>)3CH<sub>2</sub>(CH<sub>3</sub>)2NC<sub>5</sub>H<sub>3</sub>PF<sub>6</sub>
79919-53-2

(C5H5)ReNO{P(C6H5)3}(CH2(CH3)2NC5H3)(1+)*PF6(1-)=(C5H5)ReNOP(C6H5)3CH2(CH3)2NC5H3PF6

Guidance literature:
In dichloromethane; -78°C, 0.5 h under N2, addn. of 2,6-dimethylpyridine, stirring for 1 h; solvent removed under vac., solutiom warmed to room temp., orange-red residue washed with ethyl ether, redissolved in CH2Cl2, filtration through glass wool, solution layered with hexane, in the refrigerator crystd. the product;
DOI:10.1021/ja00365a027
upstream raw materials:

2,6-dimethylpyridine

tritylium hexafluorophosphate

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