benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate

Base Information

Chemical Name:benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate
CAS No.:1174020-20-2
Molecular Formula:C₇H₈O₃S*C₂₆H₃₄N₄O₄
Molecular Weight:638.785
Hs Code.:

Synonyms:benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate

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Chemical Property of benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate

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Technology Process of benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate

There total 1 articles about benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174020-68-8
C₃₆H₅₀N₄O₈

: 104-15-4
toluene-4-sulfonic acid

: 1174020-20-2
benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate

Guidance literature:: C₃₆H₅₀N₄O₈; With methanesulfonic acid; In ISOPROPYLAMIDE; at 35 - 40 ℃; for 8h;

With sodium hydroxide; In ISOPROPYLAMIDE; water; at 20 ℃;

toluene-4-sulfonic acid; In acetonitrile; at 40 ℃;

Reference yield: 94.0%

: 1174020-20-2
benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate

: 1174020-21-3
4-({[(2S,5R)-6-(benzyloxy)-7-oxo-1,6-diazabicyclo[3.2.1]octan-2-yl]carbonyl}amino)piperidine-1-carboxylic acid benzyl ester

Guidance literature:: benzyl 4-[({(2S,5R)-5-[(benzyloxy)amino]piperidin-2-yl}carbonyl)amino]piperidine-1-carboxylate mono-tosylate; With sodium hydrogencarbonate; In dichloromethane; water; for 0.5h;

With bis(trichloromethyl) carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 10 ℃; for 0.5h;