(S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

Base Information

Chemical Name:(S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide
CAS No.:1417654-08-0
Molecular Formula:C₁₇H₁₈I₂N₂O₃
Molecular Weight:552.151
Hs Code.:

Synonyms:(S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

Suppliers and Price of (S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

Chemical Property:

Purity/Quality:

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Technology Process of (S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

There total 7 articles about (S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428317-54-7
C₃₀H₃₄I₂N₂O₆

: 1417654-08-0
(S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; for 1h;

Reference yield:

: 1417654-00-2
(S)-tert-butyl (1-hydroxy-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propan-2-yl)carbamate

: 1417654-08-0
(S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide / toluene / 4.5 h / 20 °C / Cooling with ice

3: sodium azide / N,N-dimethyl-formamide / 24 h / 80 °C

4: triphenylphosphine / tetrahydrofuran; water / 18 h / 20 °C

5: pyridine / N,N-dimethyl-formamide / 0.25 h

6: triethylsilane; trifluoroacetic acid / dichloromethane / 1 h

With pyridine; triethylsilane; sodium azide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1417654-01-3
(S)-tert-butyl (1-(3,5-diiodo-4-(4-((4-methoxybenzyl)oxy)phenoxy)phenyl)-3-hydroxypropan-2-yl)carbamate

: 1417654-08-0
(S)-N-(2-amino-3-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)propyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide / toluene / 4.5 h / 20 °C / Cooling with ice

2: sodium azide / N,N-dimethyl-formamide / 24 h / 80 °C

3: triphenylphosphine / tetrahydrofuran; water / 18 h / 20 °C

4: pyridine / N,N-dimethyl-formamide / 0.25 h

5: triethylsilane; trifluoroacetic acid / dichloromethane / 1 h

With pyridine; triethylsilane; sodium azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N,N-dimethyl-formamide; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;