(cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

Base Information

Chemical Name:(cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]
CAS No.:156975-32-5
Molecular Formula:C₁₇H₂₂Cl₂NV
Molecular Weight:362.216
Hs Code.:

(cyclopentadienyl)VCl<sub>2</sub>[N-2,6-C<sub>6</sub>H<sub>3</sub>-((i)Pr)2]

Synonyms:(cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

Suppliers and Price of (cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

Chemical Property:

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Technology Process of (cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

There total 2 articles about (cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: VCl₃[N-2,6-C₆H₃-((i)Pr)2]

: 3559-74-8
trimethylsilylcyclopentadiene

: 156975-32-5
(cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

Guidance literature:: In dichloromethane; byproducts: (CH3)3SiCl; addn. of an equiv. amt. of CpSiMe3 to the V-complex in CH2Cl2; mixt. stirred (40°C, 48 h), color changed from green to golden brown; filtered, evapn. (vac.), addn. of pentane, evapn. (vac.); elem. anal.;
DOI:10.1021/om00020a003

Reference yield:

: dichloro-η(5)-cyclopentadienyl-tert-butylimido-vanadium(V)

: 24544-04-5
2,6-diisopropylbenzenamine

: 156975-32-5
(cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

Guidance literature:: In further solvent(s); byproducts: (CH3)3CNH2; 10 d at 75°C in CH2ClCH2Cl;
DOI:10.1039/a705256a

Reference yield: 67.0%

: 156975-32-5
(cyclopentadienyl)VCl₂[N-2,6-C₆H₃-((i)Pr)2]

: 594-09-2
trimethylphosphane

: 156975-33-6
(2,6-C₆H₃(i)Pr₂NVCp(PMe₃)2

Guidance literature:: With Mg; In tetrahydrofuran; mixt. of 1 equiv V-complex, 2 equiv PMe3, and a large excess of Mg in THF stirred (under Ar, room temp., 16 h); evapn. (vac.), extn. (pentane), green extract concd., cooled (-25°C, crystn. in two crops); elem. anal.;
DOI:10.1021/om00020a003