1-methylcyclohexyl diazoacetate

Base Information

Chemical Name:1-methylcyclohexyl diazoacetate
CAS No.:157944-21-3
Molecular Formula:C₉H₁₄N₂O₂
Molecular Weight:182.222
Hs Code.:

Synonyms:1-methylcyclohexyl diazoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methylcyclohexyl diazoacetate

Chemical Property:

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Technology Process of 1-methylcyclohexyl diazoacetate

There total 2 articles about 1-methylcyclohexyl diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 157944-17-7
1-methylcyclohexyl 2-diazo-3-oxobutanoate

: 157944-21-3
1-methylcyclohexyl diazoacetate

Guidance literature:: With potassium hydroxide; In acetonitrile; for 14h; Ambient temperature;
DOI:10.1002/hlca.19940770307

Reference yield:

: 91328-33-5
1-Methyl-1-cyclohexyl acetoacetate

: 157944-21-3
1-methylcyclohexyl diazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / methane sulfonyl azide, Et₃N / acetonitrile / 3 h / Ambient temperature

2: 82 percent / 8 percent KOH / acetonitrile / 14 h / Ambient temperature

With potassium hydroxide; triethylamine; Methanesulfonyl azide; In acetonitrile;
DOI:10.1002/hlca.19940770307