2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ⁵-phosphanylidene)-butane-1,4-dione

Base Information

• Chemical Name: 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ⁵-phosphanylidene)-butane-1,4-dione
• CAS No.: 134898-30-9
• Molecular Formula: C₄₁H₃₀BrO₃P
• Molecular Weight: 681.565

Synonyms:2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ⁵-phosphanylidene)-butane-1,4-dione

Chemical Property of 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ⁵-phosphanylidene)-butane-1,4-dione

Chemical Property:

Purity/Quality:

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Technology Process of 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ⁵-phosphanylidene)-butane-1,4-dione

There total 4 articles about 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ⁵-phosphanylidene)-butane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

3,3-dibromo-1,3-diphenyl-1,3-propanedione (16619-55-9) + (Benzoylmethylene)triphenylphosphorane (20913-05-7,859-65-4) → triphenylphenacylphosphonium bromide (6048-29-9) + 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ5-phosphanylidene)-butane-1,4-dione (134898-30-9)

Guidance literature:

In benzene; Heating;

Reference yield: 65.0%

(1,2-Dibenzoyl-2-bromo-3-oxo-3-phenyl-propyl)-triphenyl-phosphonium; bromide (134898-27-4) + (Benzoylmethylene)triphenylphosphorane (20913-05-7,859-65-4) → triphenylphenacylphosphonium bromide (6048-29-9) + 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ5-phosphanylidene)-butane-1,4-dione (134898-30-9)

Guidance literature:

In benzene; Heating;

Reference yield:

3,3-dibromo-1,3-diphenyl-1,3-propanedione (16619-55-9) → 2-Benzoyl-2-bromo-1,4-diphenyl-3-(triphenyl-λ5-phosphanylidene)-butane-1,4-dione (134898-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / benzene / Ambient temperature

2: 65 percent / benzene / Heating

In benzene;

upstream raw materials:

3,3-dibromo-1,3-diphenyl-1,3-propanedione

(Benzoylmethylene)triphenylphosphorane

(1,2-Dibenzoyl-2-bromo-3-oxo-3-phenyl-propyl)-triphenyl-phosphonium; bromide

Downstream raw materials:

2-benzoyl-3-bromo-1,4-diphenyl-but-2-ene-1,4-dione

triphenylphosphine

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