C₃₇H₆₆O₇Si₂

Base Information

Chemical Name:C₃₇H₆₆O₇Si₂
CAS No.:934618-05-0
Molecular Formula:C₃₇H₆₆O₇Si₂
Molecular Weight:679.098
Hs Code.:

C<sub>37</sub>H<sub>66</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₃₇H₆₆O₇Si₂

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Chemical Property of C₃₇H₆₆O₇Si₂

Chemical Property:

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Technology Process of C₃₇H₆₆O₇Si₂

There total 21 articles about C₃₇H₆₆O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 934617-82-0
C₃₅H₆₄O₆Si₂

: 108-24-7
acetic anhydride

: 934618-05-0
C₃₇H₆₆O₇Si₂

Guidance literature:: With dmap; TEA; In dichloromethane;
DOI:10.1246/cl.2007.278

Reference yield:

: 934617-86-4
C₃₇H₆₈O₆SSi₂

: 934618-05-0
C₃₇H₆₆O₇Si₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: 100 percent / TEA; DMAP / CH₂Cl₂

2.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

3.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

4.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

5.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

6.1: 65 percent / Eu(fod)3 / xylene / 120 °C

7.1: 99 percent / AgNO₃; pyridine / acetonitrile

8.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

9.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

9.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

10.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

11.1: 97 percent / DMAP; TEA / CH₂Cl₂

12.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / 50 °C

12.2: 38 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

13.1: 59 percent / n-BuLi; DIBAL / toluene

14.1: 98 percent / TEA; DMAP / CH₂Cl₂

With pyridine; quinoline; dmap; sodium tetrahydroborate; n-butyllithium; TEA; diphenyl diselenide; water; hydrogen; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278

Reference yield:

: 934618-00-5
C₃₁H₅₂O₅SSi

: 934618-05-0
C₃₇H₆₆O₇Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

2.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

3.1: 65 percent / Eu(fod)3 / xylene / 120 °C

4.1: 99 percent / AgNO₃; pyridine / acetonitrile

5.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

6.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

6.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

7.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

8.1: 97 percent / DMAP; TEA / CH₂Cl₂

9.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / 50 °C

9.2: 38 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

10.1: 59 percent / n-BuLi; DIBAL / toluene

11.1: 98 percent / TEA; DMAP / CH₂Cl₂

With pyridine; quinoline; dmap; sodium tetrahydroborate; n-butyllithium; TEA; diphenyl diselenide; hydrogen; diisobutylaluminium hydride; sodium hydrogencarbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In ethanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278