(S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester

Base Information

Chemical Name:(S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester
CAS No.:93961-03-6
Molecular Formula:C₁₅H₂₀N₂O₃
Molecular Weight:276.335
Hs Code.:

Synonyms:(S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester

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Chemical Property of (S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester

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Technology Process of (S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester

There total 8 articles about (S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 93961-02-5
(S)-3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-oxo-hexahydro-1H-azepine-1-acetic acid,phenylmethyl ester

: 93961-03-6
(S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃;
DOI:10.1016/S0960-894X(02)00010-0

Reference yield:

: 21568-87-6
2-aminocaprolactam

: 93961-03-6
(S)-3-Amino-2-oxo-hexahydro-1H-azepine-1-acetic acid, phenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / K₂CO₃ / tetrahydrofuran / 18 h / 20 °C

2.1: LiHMDS / tetrahydrofuran / 35 °C

2.2: 97 percent / tetrahydrofuran / 15 h / 0 - 20 °C

3.1: 100 percent / 5 M HCl / ethyl acetate / 0 - 20 °C

With hydrogenchloride; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/S0960-894X(02)00010-0