(2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene

Base Information

Chemical Name:(2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene
CAS No.:618457-08-2
Molecular Formula:C₃₉H₅₀O₄S
Molecular Weight:614.89
Hs Code.:

Synonyms:(2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene

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Chemical Property of (2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene

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Technology Process of (2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene

There total 1 articles about (2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 73875-18-0
(2′E)-2-(3′-methyl-4′-phenylsulfonylbut-2′-enyl)-1,4-dimethoxy-3-methylnaphthalene

: 618457-08-2
(2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at -20 ℃; for 5h;
DOI:10.1021/jo0350155

Reference yield:

: 618457-08-2
(2'E,6'E,10'E,14'E)-2-(4'-phenylsulfonyl-3',7',11',15'-tetramethylhexadeca-2',6',10',14'-tetraenyl)-1,4-dimethoxy-3-methylnaphthalene

: 863-61-6
menatetrenone

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Pd(dppe)Cl₂; LiEt₃BH / tetrahydrofuran / 1 h / 0 °C

2: 72 percent / aq. CAN / CH₂Cl₂; acetonitrile / 0.5 h / 0 °C

With ammonium cerium(IV) nitrate; (1,2-bis(diphenylphosphanyl)ethane)dichloridopalladium(II); lithium triethylborohydride; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo0350155