11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

Base Information

Chemical Name:11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one
CAS No.:1609338-15-9
Molecular Formula:C₁₇H₁₄ClN₅O
Molecular Weight:339.784
Hs Code.:

Synonyms:11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

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Chemical Property of 11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

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Technology Process of 11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

There total 6 articles about 11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1609338-14-8
N-(6-chloro-4-oxo-2-p-tolylquinazolin-3(4H)-yl)-2-hydrazinylacetamide

: 1609338-15-9
11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

Guidance literature:: With ammonium acetate; acetic acid; for 12h; Reflux;
DOI:10.1016/j.ejmech.2014.04.029

Reference yield:

: 1030524-56-1
6-chloro-2-(p-tolyl)-4H-benzo[d][1,3]oxazin-4-one

: 1609338-15-9
11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: triethylamine / dichloromethane / 12 h / 20 °C

3: hydrazine hydrate / 12 h / 20 °C

4: acetic acid; ammonium acetate / 12 h / Reflux

With ammonium acetate; hydrazine hydrate; acetic acid; triethylamine; In ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.04.029

Reference yield:

: 1246524-08-2
3-amino-6-chloro-2-p-tolylquinazolin-4(3H)-one

: 1609338-15-9
11-chloro-7-p-tolyl-2,3-dihydro-[1,2,4,5]tetrazepino[2,3-c]quinazolin-4(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 12 h / 20 °C

2: hydrazine hydrate / 12 h / 20 °C

3: acetic acid; ammonium acetate / 12 h / Reflux

With ammonium acetate; hydrazine hydrate; acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.ejmech.2014.04.029