methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate

Base Information

• Chemical Name: methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate
• CAS No.: 122775-44-4
• Molecular Formula: C₂₅H₃₁NO₆
• Molecular Weight: 441.524

Synonyms:methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate

Chemical Property of methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate

Chemical Property:

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Technology Process of methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate

There total 3 articles about methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methoxyhomophthalic anhydride (95185-43-6) → methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate (122775-44-4)

Guidance literature:

Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran; hexane / Ambient temperature

2: diethyl ether

With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;

DOI:10.1248/cpb.37.292

Reference yield:

N,N-diethyl-2,5-dimethyl-3-methoxybenzamide (122775-45-5) → methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate (122775-44-4)

Guidance literature:

Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran; hexane / Ambient temperature

2: diethyl ether

With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;

DOI:10.1248/cpb.37.292

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + {2-[2-(2-Diethylcarbamoyl-6-methoxy-4-methyl-phenyl)-acetyl]-6-methoxy-phenyl}-acetic acid → methyl 2-<ω-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)acetyl>-6-methoxyphenylacetate (122775-44-4)

Guidance literature:

In diethyl ether; Yield given;

DOI:10.1248/cpb.37.292

upstream raw materials:

diazomethane

5-methoxyhomophthalic anhydride

N,N-diethyl-2,5-dimethyl-3-methoxybenzamide

Downstream raw materials:

2-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)-5-methoxy-1,3-naphthalenediol

2-(2-N,N-diethylcarbamoyl-4-methyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

2-(3-hydroxymethoxy-1,4-dioxo-1,4-dihydro-2-naphthyl)-3-methyl-5-methoxybenzoic acid

8-hydroxy-1-methoxy-3-methyl-5H-benzonaphtho<2,3-b>pyran-5,7,12-trione

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