N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

Base Information

Chemical Name:N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester
CAS No.:142165-77-3
Molecular Formula:C₂₃H₂₆N₂O₇
Molecular Weight:442.469
Hs Code.:

Synonyms:N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

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Chemical Property of N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

Chemical Property:

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Technology Process of N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

There total 2 articles about N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2640-58-6
Nα-benzyloxycarbonyl-L-ornithine

: 142165-77-3
N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / SOCl₂ / 18 h

2: 1.) i-BuOCOCl, Et₃N / 1.) DMF, 20 min, 2.) DMF, 40 min

With thionyl chloride; triethylamine; isobutyl chloroformate;
DOI:10.1021/jm9606453

Reference yield:

: 1679-64-7
Monomethyl terephthalate

: methyl N^α-(benzyloxycarbonyl)-L-ornithinate hydrochloride

: 142165-77-3
N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

Guidance literature:: With triethylamine; isobutyl chloroformate; Yield given. Multistep reaction; 1.) DMF, 20 min, 2.) DMF, 40 min;
DOI:10.1021/jm9606453

Reference yield:

: 142165-77-3
N-((S)-4-Benzyloxycarbonylamino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

: N-((S)-4-Amino-4-methoxycarbonyl-butyl)-terephthalamic acid methyl ester

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In methanol; for 14h; under 1520 Torr;
DOI:10.1021/jm9606453